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NMR Spectroscopy. By far the most important and useful technique to identify organic molecules. Often the only technique necessary. NMR spectrum can be Nuclear magnetic resonance (NMR) spectroscopy is the study of molecular structure through measurement of the interaction of an oscillating radio-frequency NMR Spectroscopy. N.M.R. = Nuclear Magnetic Resonance. Basic Principles. Spectroscopic technique, thus relies on the interaction between material and Solid State NMR Spectroscopy: 132. The chemical shift. 132. Dipolar couplings: 135. Magic Angle Spinning (MAS). 136. Sensitivity Enhancement:.Nuclear Magnetic Resonance (NMR) Spectroscopy. 5.15 Enantiotopic and Diastereotopic Protons. 5.16 Peak Area and Proton counting : NMR Integrals. Dynamic NMR, Solid State NMR, Inorganic, Diffusion. • Spectrometer Description. – Probes and Gradients. • Structure Determination with NMR Chapter 13: Nuclear Magnetic Resonance (NMR) Spectroscopy direct observation of the H's and C's of a molecules. Nuclei are positively charged and spin on an NMR spectroscopy. Nuclear magnetic resonance (NMR) is a spec- troscopic technique that detects the energy ab- sorbed by changes in the nuclear spin state.